Effect of Water Treatment and Optimization of Extraction Applied to the Carob Pulp
Keywords:
Carob pulp, Extraction, Total sugar, OptimizationAbstract
The objective of this study was initially to determine the effect of water treatment on the chemical composition of the carob pulp. After this treatment, the pulp is devoid of most of its sugar, which makes grinding without clogging or thermal decomposition, that's what we showed in our recently patented process. The powder thus obtained, called carob pulp powder, can be used in the food industry, especially in the chocolate industry, as they contain less fat than cocoa. The aqueous extract can be used for the preparation of fruit juices, honey or carob syrup, as well as for the production of bioethanol.
In a second step the entire process of extracting sugar from the pulp was studied in this work. Thus, the response surface methodology was used to optimize the parameters of extraction was affected by the temperature, time, the ratio (L/S) (liquid/solid) and the size of the particles forming the pulp. Indeed the best optimal conditions to extract as much sugar opted for a process involving a ratio (L/S) equal to 10 for a particle size of 500 microns and a heating temperature of 60°C for 180 min.
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References
Battle I. and Tous J. : Carob tree, Ceratonia Siliqua L. International Plant Genetic Resources
Institute (IPGRI) (1997).
Gubbuk, H., Guven, D.,Gunes, E., (2009). Physical Features of some Turkish Carob (Ceratonia
Siliqua.L) pods. bull. UASVM hortic. 66. 685.
Youssif, A.K., Alghzawi,H.M. (2000). Processing and characterisation of carob powder.
food chem., 69 (2000) 283-287.
Turhan, I., Aksu, M., Karhan, M.,Tetik, N., (2006). Liquid-solid extraction of soluble solids and
Total phenolic compounds of carob bean (Ceratonia silqua L.) J.Food processEng.29, 498.
Tous, J., Romero, A., Hermose, J.F., Ninot, A., Plana, J., Battle, I., (2009).
Agronomic and commercial performance of four Spanish cultivars. Hort technology, 19,465-470.
Karkacier, M., Artik, N., Certel, M.,(1995). The conditions for carob (Ceratonia Siliqua L.)
Extraction and the clarification of the extract, fruitprocess.12, 394-397.
Ouchkif.M (1988).Etude sur le caroubier .Append number 8 of project Ouest
Srou. MARA (Morocco) GTZ (Germany), DPA of Khenifra.
Mhaisen,A.(1991).Carob tree. Agricultural Engineer, 43, 90-91.
a- Box, G. E. P. and Wilson, K.B. (1951) On the Experimental Attainment of Optimum Conditions (with
discussion). Journal of the Royal Statistical Society Series B 13(1):1–45.
b- Box, G. E. P. and Draper, Norman. (2007). Response Surfaces, Mixtures, and Ridge Analyses, Second
Edition [of Empirical Model-Building and Response Surfaces, 1987], Wiley. [10] Roseiro,J.C (1192.medium development for xantan production .process
Biochemestry, 27,167-175.
Ma, A.Y.M., and Ooraikul.B.( 1986).Optimization of enzymatic hydrolysis of carob meal
With response surface methodology. Journal of Process and preservation, 10, 99-113. [12] Kalil, S.J., maugeri,F.,and rodrigues,M.I.(2000).response surface analysis and simulation
as a tool for bioprocess design and optimization process Biochemestry,35,359-550.
a) "Traitement et Valorisation de déchets pulpe de caroube par macération, séchage et broyage pour préparer divers produits alimentaires", A. Bahloul, M. Khlifa, S. Kitane, Brevet N° 34635 (2012) déposé à l'OMPIC (Maroc).
b) Khlifa, M., Bahloul, A. Kitane, S. J. Mater. Environ. 4 (3) (2013) 348-353.
c) Khlifa, M., Bahloul, A., Kitane, S. ScienceLib Editions Mersenne, ISSN 2111-4706, Volume 5, N ° 130608,
International Standard method (ISO 928-1998). [15] Afnor Method NF V 03-905/ December (1973).
International Standard Method (ISO 8968-3-2004).
Journal Officiel de l’union Européenne, Règlement CE N°152/(2009) de la commission du
/01/2009
Journal of AOAC International. 75 (1992) 443.
Recueil des méthodes internationales d’analyses OIV (MA-AS-311-01-Sucre).1 (2009) et 2 (2011). [20] Lecoq, R. Manuel d’analyses alimentaires et d’expertises usuelles. 1 (1965) 309.
Méthode mise au point au Laboratoire de DGCCRF de Bordeaux (rapport de stage O.BEAREZ)
(1997).
Duplatre, A. Tisse, C. Etienne, J. Ann. Fals. Exp. Chim. 828 (1984) 259.
Sánchez, S.; Lozano, L.J.; GodÃnez, C.; Juan, D.; Pérez, A.; Hernández, F.J. (2010). Carob pod as
a feedstock for the production of bioethanol in Mediterranean areas. Applied Energy, 87, 3417-3424.
Haaland, P.D. "Separating signals from the noise". Experimental design in
Biotechnology (pp.61-83). New York: Marcel Dekker NY, USA, (1989).
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